2016年8月21日星期日

Ammonium Metatungstate Preparation-Neutralization Method

Ammonium metatungstate, also known as AMT, is a tungsten chemical in the form of highly soluble hydrated crystals, solubility is 303.99/loogH:O when 20℃, aqueous fairly stable. It is white or slightly yellow crystals which has no harmful components and slightly acidic.

Neutralization method with secondary ammonium metatungstate and Nitrate as the raw material purchase ammonium metatungstate: secondary ammonium metatungstate deionized water and ammonium citrate with WO3 12%~ 30% concentration of slurry. According to =1:20: nitrate ammonium paratungstate by adding 3% ~ 5% of dilute nitric acid to ammonium paratungstate slurry, control ratio of solid to liquid 1: (3 ~ 4), the Ph value of 2 ~ 4, heating and dissolving solution, the relative density of 1.18 ~ 1.20, heating to 80 ~ 90 ℃, constant temperature and constant volume control Ph value, the stirring reaction for 4H hours, aging, concentrating the supernatant to WO3 content is about 50-, filtration to remove insoluble, liquid concentration, cooling crystallization, continue to 80 ℃ drying.
ammonium metatungstate crystal
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